Zr6(L1)2(3 O)4(3 OH)4(OH)4(H2O)4 and its isostructural Hf6(L1)2(3 O)4(3 OH)4(OH)4(H2O)4 are synthesised from the linker of biphenyl 3 steroids,3′,5,5′ tetra (phenyl 4 carboxylic acid) (H4L1) and both crystallise in space group Fmmm. In comparison, the Zr6(L2)2(3 O)4(3 OH)4(OH)4(H2O)4 (denoted MFM 601) is synthesised from the amine functionalised linker of 4,4′ diamino 3,3′,5,5′ tetra(4 carboxyphenyl)biphenyl (H4L2) and crystallises in Cmmm space group. The difference in structure owes to the different conformation of the two linkers.

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